Page 168 - Handbook Bachelor Degree of Science Academic Session 20202021

Faculty of Science Handbook, Session 2019/2020

Medium of instruction: 7. A. R. Lansdown, Lubrication: a practical guide to lubricant
rd
English selection, 3 Edition. Amer Society of Mechanical
Engineers, 2003.
References: 8. R.J. Hamilton, Developments in Oils and Fats, Chapman
th
1. P. W., Atkins, Physical Chemistry, 11 ed., Oxford & Hall, 1995
University Press, New York,2018. 9. J. Boxall, Paint formulation: principles and practice,
th
2. P. W., Atkins, Molecular Quantum Mechanics, 5 ed. Industrial Pr, 1981
Oxford University Press, New York, 2008. 10. James O’connor. Standard Handbook of Lubrication
3. J. P., Lowe, Quantum Chemistry, 2 ed, Academic Engineering. 1968.
nd
Press, New York. 1993. 11. Kirk Othmer, Encyclopaedia of Chemical Technology,
4. P. W., Atkins, J. de Paula, Physical Chemistry for the 4 Edition. John Wiley & Sons, 2012.
th
Life Sciences, Oxford University Press, New York,
2006. SID3006 ADVANCED ANALYTICAL CHEMISTRY
5. Silbey, Alberty , Bawendi Physical Chemistry (Wiley),
2005. Trace Analysis

Introduction, techniques and limitations, considerations in
SID3004 INDUSTRIAL TRAINING implementation of trace analysis

Industrial training is the course designed for the B.Sc. Sample decomposition
(Applied Chemistry). Student is required to follow the Steps in total analysis, dry, wet and microwave sample
industrial training programme for a minimum of 10 weeks. digestion, appropriate considerations for decomposition of
Industrial training must be related to chemistry and the real samples.
student is required to prepare a report for evaluation. The
training programme will be briefed by the industrial training Spectrometry
programme supervisor. Atomic absorption spectroscopy, atomization techniques
including flame atomization, electrochemical atomization,
Assessment Methods: hydride technique, cold vapour technique.
Continuous assessment: 100% Atomic emission spectroscopy: arc-spark and plasma AES,
ICP-AES, atomic fluorescence spectroscopy.
Medium of instruction:
English Separation Methods
Advanced aspects on theory and process of separation in
SID3005 INDUSTRIAL CHEMISTRY II GC and HPLC, van Deemter equation, general resolution
equation and HETP, types and selection of stationary
Unit operation, principles of mass transfer, linear and radial phases in GC, capillary GC, reversed phase HPLC, effects
heat transfer based on resistance concepts to be utilized in of mobile phases in HPLC separations, instrumentation in
different types of reactor design technology. The focus will GC and HPLC, detectors in GC and HPLC, hyphenated
be on common reactor design such as batch reactor, techniques: GC-MS and LC-MS.
continuous stirred tank reactor or back-mix reactor,
fixed/suspension bed reactors, plug-flow or tubular flow
reactor and their order of important in arrangement for Electroanalytical Techniques
multiple reactors in series. Reaction engineering includes Pulse techniques in polarography, voltammetry using
mole balance equation, design equations for fractional hanging mercury drop electrode (HMDE), platinum and
conversion, reactor sizing for flow batch and flow systems. carbon electrodes. Stripping analysis-anodic stripping
Process characteristics include continuous/batch, voltammetry, trace analysis. Coulometric analysis, constant
steady/unsteady state, with/without reaction, potential coulometry, constant current coulometry,
simple/multiple reactions, yield, selectivity, applications and advantages.
desired/undesired products. Selected chemical processes
for the production of biodiesel, fatty alcohols, fatty acids, Automation
fatty amines, glycerol, ethylene glycol, soap, detergents Principles of automation, instrumental analysis, process
and surfactants. control, automatic instruments, auto-analyser,

Assessment Methods: microprocessor-controlled instruments, computers in
Continuous assessment: 30% analytical laboratories.
Final examination: 70% Assessment Methods:
Practical: 30%
Medium of instruction:
English Continuous assessment: 20%
Final examination: 50%
References: Medium of instruction:
1. R.H.Field, Chemical Engineering: Introductory Aspects, English
Houndsmills, 1988
nd
2. A.F. Mills, Heat and Mass Transfer, 2 Edition, Prentice
Hall, 1998. References: th
3. W.S. Emerson: Guide to The Chemical Industry, John 1. C. H., Daniel, Exploring Chemical Analysis, 4 ed., W.H.
Freeman Publ, 2008.
Wiley, 1983 2. G. D. Christian, Analytical Chemistry, 7 Edition, John
th
4. Fogler, H. Scott. Elements of Chemical Reaction
Engineering, 4 Edition, Prentice Hall, 2005 Wiley & Sons, 2008.
th
5. Larry D. Schmidt. The Engineering of Chemical 3. D.A. Skoog, F.J. Holler & S.R. Crouch, Principles of
th
nd
Reaction, 2 Edition, OUP USA, 2009 Instrumental Analysis, 6 ed.,Thomson Brooks/Cole,
2007
rd
6. Levenspiel, Octave. Chemical Reaction Engineering, 3 4. Harvey, D., Modern Analytical Chemistry, McGraw Hill
Edition, John Wiley & Sons, 1999
Publ, 2000.
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