Page 243 - handbook 20152016

Faculty of Science Handbook, Session 2015/2016

References: 8. Young, R. J. and Lovell, P. A. (2011), Introduction to
1. Gunstone, F. D., Harwood, J. L., Djikstra, A. J. (2007). Polymers, 3rd Ed. Taylor & Francis Group.
Lipid Handbook. 3rd Ed. CRC Press. 9. Sperling, H (1992). Introduction of Physical Polymer
2. Speight, J. G. (2006). The Chemistry and Technology of Sciences, 2nd Ed. John Wiley & Sons.
Petroleum. 4th Ed. CRC Press.
3. Gary, J. H and Handwerk, G. E. and Kaiser, M.J (2006).
Petroleum Refining: Technology and Economics. 5th
Edition. CRC Press. SID2003 BASIC ANALYTICAL CHEMISTRY
4. B.G. Reuben and M.L.Bursta (1973) The Chemical
Economy: a guide to the technology and economics of Introduction
the chemical industry, Longmans. Classical analysis, concentration systems / units, sampling
5. R.N. Shreve (1984) Shreve’s Chemical Process in analysis.
Industries, 5th ed. McGraw-Hill.
6. K. Bauer (2001) Common Fragrance and Flavor Data Treatment
materials, 3rd ed. Wiley VCH. Precision and accuracy, statistical methods for error
7. Kirk Othmer, Encyclopaedia of Chemical Technology analysis, population and sampling, confidence limits,
th
(1999-2012), 4 Edition, John Wiley and Sons. measurement uncertainty, significant figures, test for mean,
rejection of analytical data. Quality control and quality
assurance.
SID2002 INDUSTRIAL POLYMER CHEMISTRY I
Spectrometry
PART A: Polymer Synthesis Interaction of light energy between atoms and molecules;
Introduction: Basic aspects of polymers - names, chemical quantitative aspects of absorption. Molecular spectrometric
formulas/ structures and properties. Classifications of techniques – UV-Visible, IR, NIR; dispersion, absorption,
polymers, thermoplastics, thermosets and elastomers. fluorescence and emission. Spectrophotometric
Requirements of selective industries surface coatings, instruments; emission spectroscopy and atomic absorption
adhesives, packaging, automotives, construction and spectrometry- an introduction, uses of spectrophotometry.
medical appliances. Discussion about the management of
polymers in the environment. Polymerisations: Mechanism, Electroanalytical Chemistry
basic polymerisations (step-growth dan chain-growth), Quantitative analysis – standard addition technique and
advanced synthesis techniques (introduction of controlled internal standard technique, Potentiometry – pH glass
living radical polymerisations) and industrial polymerisation electrode, solid membrane ion selective electrodes.
processes (bulk, solution, suspension, emulsion, solid-state, Heyrovsky equation.
gas phase and plasma polymerisation and polymerization in Separation Methods
supercritical fluid). Measurement of molecular weight: Basic Introduction to the theory and process of separation in GC
introduction on molecule weight, MW and molecular weight and HPLC, ion exchange chromatography, solvent
distribution, MWD, also effects on the physical properties of extraction, partition coefficient, multiple extraction,
polymers. efficiency.

PART B: Latex and Rubber Equilibria
Type of latices: natural, synthetic, artificial and modified Important equilibria in analytical chemistry, acid-base
latices. Latex composition. Latex testing (Physical tests: dry equilibria, calculating pH of buffer solutions, acid-base
rubber content (DRC) and total solid content of latex (TSC); titration curves.
Chemical tests: protein analysis; stability test). Latex
applications: dipping, extrusion and foam. Rubber: Complexometric titrations and metal speciation
Introduction on the SMR grades. Vulcanised rubber. Rubber Metal complex equilibria, EDTA – the ligand and its
testing (e.g. tensile, hardness, abrasion etc), Rubber complexes, selectivity via control of pH, selectivity via
applications: tyres, footwear etc.) Viscoelasticity: masking agent, applications of EDTA.
Introduction, dynamic-mechanical analysis, viscoelastic
properties of polymer solutions and melts, dielectric Assessment Methods:
analysis. Rubber elasticity: Thermodynamics and statistical Continuous assessment: 20%
theory, phenomenological model and recent development. Practical: 30%
Mechanical properties of polymers – measurements of Final examination: 50%
mechanical properties: tensile, elongation, modulus etc.
Medium of instruction:
Assessment Methods: English
Continuous assessment: 20%
Practical: 30% Soft skills:
Final examination: 50% CT1 – 3, TS1

Medium of instruction: References:
English 7. D.A. Skoog, D.M. West, F.J. Holler & S.R Crouch,
Fundamentals of Analytical Chemistry, 9th Ed., 2014,
Soft skills: Thomson, Brooks/ Cole.
CT1 – 3 8. Francis Rouessac & Annick Roussac, Chemical Analysis-
Modern Instrumental Methods and Techniques, 4th Ed.,
References: 2010, John Wiley & Sons.
6. Fried, J. R. (2003), Polymer Science & Technology, 2nd 9. G. D. Christian, Analytical Chemistry, 6th Ed, 2010 John
Ed. Prentice Hall. Wiley & Son.
7. Flory, P. J. (1991), Prinsip Kimia Polimer (Terjemahan),
Dewan Bahasa dan Pustaka.

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