Page 248 - handbook 20152016

Faculty of Science Handbook, Session 2015/2016

4. Atkins, P. W., de Paula, J. (2006). Physical Chemistry for 10. James O’connor. Standard Handbook of Lubrication
the Life Sciences, Oxford University Press, New York. Engineering. 1968.
5. Silbey, Alberty & Bawendi (2005), Physical Chemistry 11. Kirk Othmer, Encyclopaedia of Chemical Technology,
th
(Wiley). 4 Edition. John Wiley & Sons, 2012.

SID3004 INDUSTRIAL TRAINING SID3006 ADVANCED ANALYTICAL CHEMISTRY

Industrial training is the course designed for the B.Sc. Trace Analysis
(Applied Chemistry). Student is required to follow the
industrial training programme for a minimum of 10 weeks. Introduction, techniques and limitations, considerations in
Industrial training must be related to chemistry and the implementation of trace analysis
student is required to prepare a report for evaluation. The
training programme will be briefed by the industrial training Sample decomposition
programme supervisor. Steps in total analysis, dry, wet and microwave sample
digestion, appropriate considerations for decomposition of
Assessment Methods: real samples.
Continuous assessment: 100%
Spectrometry
Medium of instruction: Atomic absorption spectroscopy, atomization techniques
English including flame atomization, electrochemical atomization,
hydride technique, cold vapour technique.
Soft skills: Atomic emission spectroscopy: arc-spark and plasma AES,
CT1 – 3, CS1 – 3, TS1 – 2, EM1 – 2 ICP-AES, atomic fluorescence spectroscopy.

SID3005 INDUSTRIAL CHEMISTRY II Separation Methods
Advanced aspects on theory and process of separation in
Unit operation, principles of mass transfer, linear and radial GC and HPLC, van Deemter equation, general resolution
heat transfer based on resistance concepts to be utilized in equation and HETP, types and selection of stationary
different types of reactor design technology. The focus will phases in GC, capillary GC, reversed phase HPLC, effects
be on common reactor design such as batch reactor, of mobile phases in HPLC separations, instrumentation in
continuous stirred tank reactor or back-mix reactor, GC and HPLC, detectors in GC and HPLC, hyphenated
fixed/suspension bed reactors, plug-flow or tubular flow techniques: GC-MS and LC-MS.
reactor and their order of important in arrangement for
multiple reactors in series. Reaction engineering includes Electroanalytical Techniques
mole balance equation, design equations for fractional Pulse techniques in polarography, voltammetry using
conversion, reactor sizing for flow batch and flow systems. hanging mercury drop electrode (HMDE), platinum and
Process characteristics include continuous/batch,
steady/unsteady state, with/without reaction, simple/multiple carbon electrodes. Stripping analysis-anodic stripping
reactions, yield, selectivity, desired/undesired products. voltammetry, trace analysis. Coulometric analysis, constant
Selected chemical processes for the production of biodiesel, potential coulometry, constant current coulometry,
applications and advantages.
fatty alcohols, fatty acids, fatty amines, glycerol, ethylene
glycol, soap, detergents and surfactants.
Automation
Assessment Methods: Principles of automation, instrumental analysis, process
Continuous assessment: 30% control, automatic instruments, auto-analyser,
Final examination: 70% microprocessor-controlled instruments, computers in
analytical laboratories.
Medium of instruction:
English Assessment Methods:
Practical: 30%
Soft skills: Continuous assessment: 20%
CT1 – 3, KK1, LL1 – 2 Final examination: 50%

References: Medium of instruction:
1. R.H.Field, Chemical Engineering: Introductory Aspects, English
Houndsmills, 1988
nd
2. A.F. Mills, Heat and Mass Transfer, 2 Edition, Soft skills:
Prentice Hall, 1998. CT1 – 3, CS1 – 3, LL1 – 2
3. W.S. Emerson: Guide to The Chemical Industry, John
Wiley, 1983 References:
4. Fogler, H. Scott. Elements of Chemical Reaction 1. Daniel C. Harris, Exploring Chemical Analysis, 4
th
th
Engineering, 4 Edition, Prentice Hall, 2005 Ed.,W.H. Freeman Publ, 2008
th
5. Larry D. Schmidt. The Engineering of Chemical 2. G. D. Christian, Analytical Chemistry, 7 Edition, John
nd
Reaction, 2 Edition, OUP USA, 2009 Wiley & Sons, 2008
6. Levenspiel, Octave. Chemical Reaction Engineering, 3. D.A. Skoog, F.J. Holler & S.R. Crouch, Principles of
rd
3 Edition, John Wiley & Sons, 1999 Instrumental Analysis, 6 Ed.,Thomson Brooks/Cole,
th
7. A. R. Lansdown, Lubrication: a practical guide to 2007
rd
lubricant selection, 3 Edition. Amer Society of 4. David Harvey, Modern Analytical Chemistry, McGraw Hill
Mechanical Engineers, 2003. Publ, 2000
8. R.J. Hamilton, Developments in Oils and Fats, 5. D.A. Skoog, D.M. West, F.J. Holler & S.R. Crouch,
th
Chapman & Hall, 1995 Fundamentals of Analytical Chemistry, 8 Ed.,
9. J. Boxall, Paint formulation: principles and practice, Brooks/Cole Publ, 2004.
Industrial Pr, 1981
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