Page 192 - handbook 20162017
P. 192

Faculty of Science Handbook, Session 2016/2017

               commercially useful products. Challenges on the synthesis  Latex  applications:  dipping,  extrusion  and  foam.  Rubber:
               of chemicals that are beneficial, profitable and responsible  Introduction  on  the  SMR  grades.  Vulcanised  rubber.
               for  the  safety,  health  and  environment.    Research  and  Rubber  testing  (e.g.  tensile,  hardness,  abrasion  etc),
               development from laboratory scale to commercial scale on  Rubber  applications:  tyres,  footwear  etc.)  Viscoelasticity:
               the  production  of  selected  chemicals.  Economic  aspect,  Introduction,  dynamic-mechanical  analysis,  viscoelastic
               fixed cost, variable cost, revenue, management and patent  properties  of  polymer  solutions  and  melts,  dielectric
               right. Forecasting the profitability for pioneering industries  analysis.    Rubber  elasticity:  Thermodynamics  and
               on  the  production  of  selected  chemicals  through  statistical  theory,  phenomenological  model  and  recent
               interpretation of break-even chart.            development.  Mechanical  properties  of  polymers  –
                                                              measurements   of   mechanical   properties:   tensile,
               Separation technology covers aspects related to chemical  elongation, modulus etc.
               process  of  adsorption,  extraction,  purification  and
               distillation.  The  chemical  process  includes  natural  gas,  Assessment Methods:
               petroleum and vegetable oil.                   Continuous assessment:  20%
                                                              Practical:           30%
               Petroleum  refining  process  includes  crude  oil  distillation,  Final examination:  50%
               delayed  coking,  catalytic  reforming  and  isomerisation,
               cracking  and  hydrotreating.  Palm  oil  refining  includes  Medium of instruction:
               physical  and  chemical  processes  on  upstream  and  English
               downstream industries.
                                                              Soft skills:
               Assessment Methods:                            CT1 – 3
               Continuous assessment:  30%
               Final examination:    70%                      References:
                                                              1.  Fried,  J.  R.  (2003),  Polymer  Science  &  Technology,
               Medium of instruction:                          2nd
               English                                         Ed. Prentice Hall.
                                                              2.      Flory,  P.  J.  (1991),  Prinsip  Kimia  Polimer
               Soft skills:                                    (Terjemahan), Dewan Bahasa dan Pustaka.
               CT1 – 3, LL1 – 2, CS1 – 3                      3.      Young, R.  J. and Lovell,  P.  A. (2011),
                                                               Introduction  to  Polymers,  3rd  Ed. Taylor  &  Francis
               References:                                     Group.
               1. Gunstone, F. D., Harwood, J. L., Djikstra, A. J. (2007).  4.  Sperling,  H  (1992).  Introduction  of  Physical
                 Lipid Handbook. 3rd Ed. CRC Press.            Polymer Sciences, 2nd Ed. John Wiley & Sons.
               2. Speight, J. G. (2006). The Chemistry and Technology of
                 Petroleum. 4th Ed. CRC Press.
               3. Gary, J. H and Handwerk, G. E. and Kaiser, M.J (2006).
                 Petroleum  Refining:  Technology  and  Economics.  5th  SID2003 BASIC ANALYTICAL CHEMISTRY
                 Edition. CRC Press.
               4. B.G.  Reuben  and  M.L.Bursta  (1973)  The  Chemical  Introduction
                 Economy: a guide to the technology and economics of  Classical analysis, concentration systems / units, sampling
                 the chemical industry, Longmans.             in analysis.
               5.  R.N.  Shreve  (1984)  Shreve’s  Chemical  Process  Data Treatment
                 Industries, 5th ed. McGraw-Hill.             Precision  and  accuracy,  statistical  methods  for  error
               6.  K.  Bauer  (2001)  Common  Fragrance  and  Flavor  analysis,  population  and  sampling,  confidence  limits,
                 materials, 3rd ed. Wiley VCH.                measurement  uncertainty,  significant  figures,  test  for
               7.  Kirk Othmer, Encyclopaedia of Chemical Technology  mean,  rejection  of  analytical  data.  Quality  control  and
                            th
                 (1999-2012), 4 Edition, John Wiley and Sons.  quality assurance.
                                                              Spectrometry
               SID2002 INDUSTRIAL POLYMER CHEMISTRY I         Interaction of light energy between atoms and molecules;
                                                              quantitative   aspects   of   absorption.   Molecular
               PART A: Polymer Synthesis                      spectrometric  techniques  –  UV-Visible,  IR,  NIR;
               Introduction: Basic aspects of polymers - names, chemical  dispersion,  absorption,  fluorescence  and  emission.
               formulas/  structures  and  properties.  Classifications  of  Spectrophotometric  instruments;  emission  spectroscopy
               polymers,  thermoplastics,  thermosets  and  elastomers.  and atomic absorption spectrometry- an introduction, uses
               Requirements  of  selective  industries  surface  coatings,  of spectrophotometry.
               adhesives,  packaging,  automotives,  construction  and
               medical appliances. Discussion about the management of  Electroanalytical Chemistry
               polymers   in   the   environment.   Polymerisations:  Quantitative  analysis – standard  addition  technique  and
               Mechanism,  basic  polymerisations  (step-growth  dan  internal  standard  technique,  Potentiometry – pH  glass
               chain-growth),   advanced   synthesis   techniques  electrode,  solid  membrane  ion  selective  electrodes.
               (introduction  of  controlled  living  radical  polymerisations)  Heyrovsky equation.
               and  industrial  polymerisation  processes  (bulk,  solution,  Separation Methods
               suspension, emulsion, solid-state, gas phase and plasma  Introduction to the theory and process of separation in GC
               polymerisation  and  polymerization  in  supercritical  fluid).  and  HPLC,  ion  exchange  chromatography,  solvent
               Measurement  of  molecular  weight:  Basic  introduction  on  extraction,  partition  coefficient,  multiple  extraction,
               molecule  weight,  MW  and  molecular  weight  distribution,  efficiency.
               MWD, also effects on the physical properties of polymers.
                                                              Equilibria
               PART B: Latex and Rubber                       Important  equilibria  in  analytical  chemistry,  acid-base
               Type  of  latices:  natural,  synthetic,  artificial  and  modified  equilibria,  calculating  pH  of  buffer  solutions,  acid-base
               latices.  Latex  composition.  Latex  testing  (Physical  tests:  titration curves.
               dry rubber content (DRC) and total solid content of latex
               (TSC); Chemical  tests:  protein  analysis;  stability  test).  Complexometric titrations and metal speciation


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