Page 188 - tmp

Faculty of Science Handbook, Session 2017/2018

Separation technology covers aspects related to chemical measurements of mechanical properties: tensile,
process of adsorption, extraction, purification and elongation, modulus etc.
distillation. The chemical process includes natural gas,
petroleum and vegetable oil. Assessment Methods:
Continuous assessment: 20%
Petroleum refining process includes crude oil distillation, Practical: 30%
delayed coking, catalytic reforming and isomerisation, Final examination: 50%
cracking and hydrotreating. Palm oil refining includes
physical and chemical processes on upstream and Medium of instruction:
downstream industries. English
Assessment Methods: Soft skills:
Continuous assessment: 30% CT1 – 3
Final examination: 70%
References:
Medium of instruction: 1.Fried, J. R. (2003), Polymer Science & Technology, 2nd
English Ed. Prentice Hall.
2.Flory, P. J. (1991), Prinsip Kimia Polimer (Terjemahan),
Soft skills: Dewan Bahasa dan Pustaka.
CT1 – 3, LL1 – 2, CS1 – 3 3.Young, R. J. and Lovell, P. A. (2011), Introduction to
Polymers, 3rd Ed. Taylor & Francis Group.
References: 4.Sperling, H (1992). Introduction of Physical Polymer
1. Gunstone, F. D., Harwood, J. L., Djikstra, A. J. (2007). Sciences, 2nd Ed. John Wiley & Sons.
Lipid Handbook. 3rd Ed. CRC Press.
2. Speight, J. G. (2006). The Chemistry and Technology of
Petroleum. 4th Ed. CRC Press. SID2003 BASIC ANALYTICAL CHEMISTRY
3. Gary, J. H and Handwerk, G. E. and Kaiser, M.J (2006).
Petroleum Refining: Technology and Economics. 5th Introduction
Edition. CRC Press. Classical analysis, concentration systems / units, sampling
4. B.G. Reuben and M.L.Bursta (1973) The Chemical in analysis.
Economy: a guide to the technology and economics of Data Treatment
the chemical industry, Longmans. Precision and accuracy, statistical methods for error
5. R.N. Shreve (1984) Shreve’s Chemical Process analysis, population and sampling, confidence limits,
Industries, 5th ed. McGraw-Hill. measurement uncertainty, significant figures, test for
6. K. Bauer (2001) Common Fragrance and Flavor mean, rejection of analytical data. Quality control and
materials, 3rd ed. Wiley VCH. quality assurance.
7. Kirk Othmer, Encyclopaedia of Chemical Technology
(1999-2012), 4 Edition, John Wiley and Sons. Spectrometry
th
Interaction of light energy between atoms and molecules;
quantitative aspects of absorption. Molecular
SID2002 INDUSTRIAL POLYMER CHEMISTRY I spectrometric techniques – UV-Visible, IR, NIR;
dispersion, absorption, fluorescence and emission.
PART A: Polymer Synthesis Spectrophotometric instruments; emission spectroscopy
Introduction: Basic aspects of polymers - names, chemical and atomic absorption spectrometry- an introduction, uses
formulas/ structures and properties. Classifications of of spectrophotometry.
polymers, thermoplastics, thermosets and elastomers.
Requirements of selective industries surface coatings, Electroanalytical Chemistry
adhesives, packaging, automotives, construction and Quantitative analysis – standard addition technique and
medical appliances. Discussion about the management of internal standard technique, Potentiometry – pH glass
polymers in the environment. Polymerisations: electrode, solid membrane ion selective electrodes.
Mechanism, basic polymerisations (step-growth dan Heyrovsky equation.
chain-growth), advanced synthesis techniques Separation Methods
(introduction of controlled living radical polymerisations) Introduction to the theory and process of separation in GC
and industrial polymerisation processes (bulk, solution, and HPLC, ion exchange chromatography, solvent
suspension, emulsion, solid-state, gas phase and plasma extraction, partition coefficient, multiple extraction,
polymerisation and polymerization in supercritical fluid). efficiency.
Measurement of molecular weight: Basic introduction on
molecule weight, MW and molecular weight distribution, Equilibria
MWD, also effects on the physical properties of polymers. Important equilibria in analytical chemistry, acid-base
equilibria, calculating pH of buffer solutions, acid-base
PART B: Latex and Rubber titration curves.
Type of latices: natural, synthetic, artificial and modified
latices. Latex composition. Latex testing (Physical tests: Complexometric titrations and metal speciation
dry rubber content (DRC) and total solid content of latex Metal complex equilibria, EDTA – the ligand and its
(TSC); Chemical tests: protein analysis; stability test). complexes, selectivity via control of pH, selectivity via
Latex applications: dipping, extrusion and foam. Rubber: masking agent, applications of EDTA.
Introduction on the SMR grades. Vulcanised rubber.
Rubber testing (e.g. tensile, hardness, abrasion etc), Assessment Methods:
Rubber applications: tyres, footwear etc.) Viscoelasticity: Practical: 30%
Introduction, dynamic-mechanical analysis, viscoelastic Continuous assessment: 20%
properties of polymer solutions and melts, dielectric Final examination: 50%
analysis. Rubber elasticity: Thermodynamics and
statistical theory, phenomenological model and recent Medium of instruction:
development. Mechanical properties of polymers – English

184