Page 173 - buku panduan 20192020

Faculty of Science Handbook, Session 2019/2020

Assessment Methods: Soft skills:
Practical: 25% CT1-3
Continuous assessment: 15%
Final examination: 60% References:
1. D. A. Skoog, D. M. West, F.J. Holler & S.R Crouch,
th
Medium of instruction: Fundamentals of Analytical Chemistry, 9 ed., Cengage,
English Brooks/ Cole, 2014.
2. Francis Rouessac & Annick Roussac, Chemical
Soft skills: Analysis-Modern Instrumental Methods and Techniques,
CT1-3 4 ed., John Wiley & Sons, 2010.
th
3. G. D. Christian, Analytical Chemistry, 7 ed., John Wiley
th
References: & Son, 2013.
h
1. P. W. Atkins, Physical Chemistry, 11 ed., Oxford 4. D. L. Robert, Aqueous acid-base equilibria and titrations,
University Press, 2018. Oxford: Oxford University Press, 1999.
2. Donald A. McQuarrie, Quantum Chemistry, University 5. S. Gerold, Complexometric titrations, London : Methuen,
Science Book, 1983 1969.
nd
3. F. J. Bockhoff, Elements of Quantum Theory, 2 ed., 6. I.S. Krull, Trace metal analysis and speciation,
Addison-Wesley Pub. Company, 1976. Amsterdam : Elsevier, 1991.
4. G. M. Barrow, Physical Chemistry, 6 ed., McGraw-Hill, 7. D.C. Harris, Quantitative Chemical Analysis, 9 ed., WH
th
th
1996. Freeman, 2015.
5. R. A. Alberty & R. J. Silbey, Physical Chemistry, 4 ed.,
th
John Wiley, 2010.
SIC2005 POLYMER CHEMISTRY I

SIC2004 ANALYTICAL CHEMISTRY I Fundamental polymer chemistry
Classification and naming. Processes of polymer
Introduction synthesis: bulk, solution, suspension and emulsion.
Classical analysis, concentration systems / units, sampling Mechanisms of polymerization: condensation, Carothers
in analysis. Equations, radical, ionic (cationic and anionic).
Copolymerization: structures and properties of
Data Treatment copolymers, reactivity ratios. Thermosets: fenoplast,
Precision and accuracy, statistical methods for error aminoplast, unsaturated polyesters, polyurethanes epoxy
analysis, population and sampling, confidence limits, resins. Relationship between structure and properties:
measurement uncertainty, significant figures, test for structural isomers, stereospecific vinyl polymers, and
mean, rejection of analytical data. Quality control and structures of polymers from diene monomers and ways to
quality assurance. overcome or reduce the problems of environmental
pollutions.
Spectrometry
Interaction of light energy between atoms and molecules; Physical chemistry of polymers
quantitative aspects of absorption. Molecular Simple kinetic of radical polymerization. Introduction to the
spectrometric techniques – UV-Visible, IR, NIR; size and conformation of polymer chain. Polymer in
dispersion, absorption, fluorescence and emission. solution– interaction between solvent and polymer
Spectrophotometric instruments; emission spectroscopy molecules. Effect of molecular weight on the physical
and atomic absorption spectrometry- an introduction, uses properties of polymers. Distribution of molecular weights
of spectrophotometry. and average molecular weights M n and M v. Determination
of average molecular weight: (a) end-group analysis, (b)
Electroanalytical Chemistry osmometry, (c) viscometry.
Quantitative analysis – standard addition technique and
internal standard technique, Potentiometry – pH glass Assessment Methods:
electrode, solid membrane ion selective electrodes. Practical: 30%
Heyrovsky equation. Continuous assessment: 20%
Final examination: 50%
Separation Methods
Introduction to the theory and process of separation in GC Medium of instruction:
and HPLC, ion exchange chromatography, solvent English
extraction, partition coefficient, multiple extraction,
efficiency. Soft skills:
CT1-3
Equilibria
Important equilibria in analytical chemistry, acid-base References:
equilibria, calculating pH of buffer solutions, acid-base 1. Joel R. Fried, Polymer Science and Technology, 3 ed.,
rd
titration curves. Prentice Hall International Editions, 2011.
2. R. A, Harry & W. L. Frederick, Contemporary Polymer
Complexometric titrations and metal speciation Chemistry, 3 ed., Prentice Hall, 2010.
rd
rd
Metal complex equilibria, EDTA – the ligand and its 3. M. P. Steven, Polymer Chemistry – An Introduction, 3
complexes, selectivity via control of pH, selectivity via ed., Oxford Univ. Press, 2010.
masking agent, applications of EDTA. 4. G. Challa, Polymer Chemistry - an Introduction, Ellis
Horwood, 2010.
Assessment Methods: 5. L. R. Stephen, Fundamental principles of polymeric
rd
Practical: 30% materials, 3 ed., John Wiley, 2010.
Continuous assessment: 20%
Final examination: 50%

Medium of instruction:
English
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